(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

Base Information

Chemical Name:(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine
CAS No.:93062-04-5
Molecular Formula:C₂₀H₂₄N₂O₄S₃
Molecular Weight:452.62
Hs Code.:

Synonyms:(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

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Chemical Property of (+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

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Technology Process of (+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

There total 3 articles about (+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 93133-33-6
3,6-dimethyl-2-(toluene-4-sulfonyl)-1-(toluene-4-sulfonylimino)-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

: 93062-04-5
(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

Guidance literature:: In benzene; for 1h; Heating;
DOI:10.1021/ja00337a037

Reference yield:

: 4104-47-6
N-sulfinyl-p-toluenesulfonamide

: 93062-04-5
(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / benzene / 1 h / Ambient temperature

2: 48 percent / benzene / 15 h / Ambient temperature

3: 100 percent / benzene / 1 h / Heating

With pyridine; In benzene;
DOI:10.1021/ja00337a037

Reference yield:

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 93062-04-5
(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / benzene / 15 h / Ambient temperature

2: 100 percent / benzene / 1 h / Heating

In benzene;
DOI:10.1021/ja00337a037