3,5-Diethoxyisonicotinaldehyde

Base Information

• Chemical Name: 3,5-Diethoxyisonicotinaldehyde
• CAS No.: 164077-50-3
• Molecular Formula: C10H13 N O3
• Molecular Weight: 195.22
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID00704430
• Nikkaji Number: J3.028.282E
• Wikidata: Q82636852
• Mol file: 164077-50-3.mol

Synonyms:3,5-Diethoxyisonicotinaldehyde;164077-50-3;3,5-diethoxypyridine-4-carbaldehyde;3,5-Diethoxypyridine-4-carboxaldehyde;DTXSID00704430;AKOS006308096;SB54566;FT-0733203

Chemical Property of 3,5-Diethoxyisonicotinaldehyde

Chemical Property:

• Boiling Point: 341.9±37.0 °C(Predicted)
• PKA: 2.22±0.10(Predicted)
• PSA: 48.42000
• Density: 1.113±0.06 g/cm3(Predicted)
• LogP: 1.69150
• Storage Temp.: 2-8°C
• XLogP3: 1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 195.08954328
• Heavy Atom Count: 14
• Complexity: 161

Purity/Quality:

98%min ^*data from raw suppliers

3,5-diethoxyisonicotinaldehyde 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC1=CN=CC(=C1C=O)OCC

Technology Process of 3,5-Diethoxyisonicotinaldehyde

There total 1 articles about 3,5-Diethoxyisonicotinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-diethoxypyridine (98959-85-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3,5-diethoxy-4-pyridinecarboxaldehyde (164077-50-3)

Guidance literature:

With methyllithium; Yield given. Multistep reaction; 1.) THF, ether, RT, 4 h, 2.) THF, ether, 40 min;

DOI:10.3987/COM-94-6945

upstream raw materials:

3,5-diethoxypyridine

N,N-dimethyl-formamide

Refernces