ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

Base Information

Chemical Name:ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate
CAS No.:1136839-31-0
Molecular Formula:C₁₆H₂₁ClO₆
Molecular Weight:344.792
Hs Code.:

Synonyms:ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

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Technology Process of ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

There total 2 articles about ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 89048-25-9
2,3,4,5-tetramethoxy-6-methyl benzaldehyde

: 1136839-31-0
ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

Guidance literature:: ethyl 2-diethoxyphosphorylpropionate; With sodium hydride; In toluene; at 20 ℃; Inert atmosphere;

2,3,4,5-tetramethoxy-6-methyl benzaldehyde; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/jm9014857

Reference yield:

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 1136839-30-9
2-chloro-3,4,5,6-tetramethoxybenzaldehyde

: ethyl (Z)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

: 1136839-31-0
ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

Guidance literature:: ethyl 2-diethoxyphosphorylpropionate; With sodium hydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

2-chloro-3,4,5,6-tetramethoxybenzaldehyde; In tetrahydrofuran; at 20 ℃; for 12h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jm9014857

Reference yield: 95.0%

: 1136839-31-0
ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate

: 1136839-29-6
C₁₄H₁₇ClO₆

Guidance literature:: ethyl (E)-3-(2-chloro-3,4,5,6-tetramethoxyphenyl)-2-methyl-2-propenoate; With potassium hydroxide; In ethanol; for 0.5h; Reflux; Inert atmosphere;

With hydrogenchloride; water; In ethanol;
DOI:10.1021/jm9014857