N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide

Base Information

• Chemical Name: N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide
• CAS No.: 906342-14-1
• Molecular Formula: C₂₈H₂₄N₂O₄
• Molecular Weight: 452.51

Synonyms:N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide

Chemical Property of N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide

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Technology Process of N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide

There total 3 articles about N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionic acid → N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide (906342-14-1)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / N,N-dimethyl-acetamide / -10 °C

2: N,N-dimethyl-acetamide / 20 °C

With thionyl chloride; In N,N-dimethyl acetamide;

DOI:10.1021/jm060302x

Reference yield:

1-furan-2-yl-2-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-ethanone → N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide (906342-14-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: O₃ / methanol / -78 °C

1.2: dimethyl sulfide / methanol / 20 °C

1.3: KOH / methanol

2.1: SOCl₂ / N,N-dimethyl-acetamide / -10 °C

3.1: N,N-dimethyl-acetamide / 20 °C

With thionyl chloride; ozone; In methanol; N,N-dimethyl acetamide;

DOI:10.1021/jm060302x

Reference yield:

6-amino-4-methyl-2,3-benzoxazin-1-one (217196-94-6) + 2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionyl chloride → N-(4-methyl-1-oxo-1H-benzo[d][1,2]oxazin-6-yl)-2-oxo-3-(1-phenyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-propionamide (906342-14-1)

Guidance literature:

In N,N-dimethyl acetamide; at 20 ℃;

DOI:10.1021/jm060302x

upstream raw materials:

6-amino-4-methyl-2,3-benzoxazin-1-one

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