ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside
CAS No.:1240564-09-3
Molecular Formula:C₂₉H₃₈O₆S
Molecular Weight:514.683
Hs Code.:

Synonyms:ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

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Technology Process of ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

There total 1 articles about ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1240564-07-1
ethyl 4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

: 106-95-6
allyl bromide

: 1240564-09-3
ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.75h;
DOI:10.1016/j.carres.2010.03.006

Reference yield: 90.0%

: 1240564-09-3
ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

: 1240564-10-6
ethyl 6-O-allyl-4,7-di-O-benzyl-1-thio-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With acetic acid; In water; at 80 ℃; for 2h;
DOI:10.1016/j.carres.2010.03.006

Reference yield: 52.0%

: 1240564-09-3
ethyl 6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-1-thio-L-glycero-α-D-manno-heptopyranoside

: 215381-22-9
(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->4)-7-O-acetyl-1,6-anhydro-2-O-benzyl-L-glycero-β-D-manno-heptopyranose

: 1240564-12-8
6-O-allyl-4,7-di-O-benzyl-2,3-O-isopropylidene-L-glycero-β-D-manno-heptopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)]-7-O-acetyl-1,6-anhydro-2-O-benzyl-L-glycero-α-D-manno-heptopyranose

Guidance literature:: With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In diethyl ether; at 0 - 20 ℃; for 2h; regioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.carres.2010.03.006