3-phenyl-2-propynal triisopropylhydrazone

Base Information

Chemical Name:3-phenyl-2-propynal triisopropylhydrazone
CAS No.:1175531-19-7
Molecular Formula:C₁₈H₂₈N₂Si
Molecular Weight:300.519
Hs Code.:

Synonyms:3-phenyl-2-propynal triisopropylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenyl-2-propynal triisopropylhydrazone

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Technology Process of 3-phenyl-2-propynal triisopropylhydrazone

There total 1 articles about 3-phenyl-2-propynal triisopropylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2579-22-8
Phenylpropargyl aldehyde

: 285128-78-1
triisopropylsilyl hydrazine

: 1175531-19-7
3-phenyl-2-propynal triisopropylhydrazone

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 2.5h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol9010932

Reference yield:

: 1175531-19-7
3-phenyl-2-propynal triisopropylhydrazone

: 157022-40-7
(3-diazoprop-1-yn-1-yl)benzene

Guidance literature:: 3-phenyl-2-propynal triisopropylhydrazone; With tetrabutyl ammonium fluoride; In tetrahydrofuran; Inert atmosphere;

With lead(IV) tetraacetate; N,N,N',N'-tetramethylguanidine; In N,N-dimethyl-formamide; at -45 ℃; Inert atmosphere;
DOI:10.1021/ol9010932