C₃₁H₃₆O₆

Base Information

Chemical Name:C₃₁H₃₆O₆
CAS No.:1354747-45-7
Molecular Formula:C₃₁H₃₆O₆
Molecular Weight:504.623
Hs Code.:

C<sub>31</sub>H<sub>36</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₆O₆

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Chemical Property of C₃₁H₃₆O₆

Chemical Property:

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Technology Process of C₃₁H₃₆O₆

There total 10 articles about C₃₁H₃₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 201279-58-5
1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

: 1354747-45-7
C₃₁H₃₆O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanol; sodium methylate / 1 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

6.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

7.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

7.2: 20 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

8.2: 24 h / -40 - -20 °C / Inert atmosphere

9.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

10.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

With 1H-imidazole; titanium(IV) isopropylate; methanol; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; tetrabutyl ammonium fluoride; iodine; sodium methylate; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; zinc; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; benzene; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ol2032448

Reference yield:

: 1354747-41-3
C₃₁H₃₆O₅

: 1354747-45-7
C₃₁H₃₆O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

1.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

3.2: 24 h / -40 - -20 °C / Inert atmosphere

4.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

5.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

With 1H-imidazole; titanium(IV) isopropylate; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; iodine; sodium methylate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; zinc; In methanol; diethyl ether; ethanol; dichloromethane; benzene; 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1021/ol2032448

Reference yield:

: C₃₁H₃₆O₇

: 1354747-45-7
C₃₁H₃₆O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

2: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

With 1H-imidazole; iodine; triphenylphosphine; zinc; In diethyl ether; ethanol; benzene;
DOI:10.1021/ol2032448