9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

Base Information

Chemical Name:9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one
CAS No.:140679-73-8
Molecular Formula:C₃₀H₂₈N₄O₅
Molecular Weight:524.576
Hs Code.:

Synonyms:9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

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Chemical Property of 9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

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Technology Process of 9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

There total 6 articles about 9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 140679-72-7
2,2-Dimethyl-propionic acid (2R,3R,4R,5R)-4-methanesulfonyloxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-2-(6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yl ester

: 140679-73-8
9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

Guidance literature:: With potassium hydroxide; sodium tetrahydroborate; In methanol; benzene; for 27.5h; Ambient temperature;
DOI:10.1039/P19920000469

Reference yield: 9.0%

: 140701-68-4
5'-O-(4-methoxytrityl)-2',3'-bis-O-methylsulfonylinosine

: 140679-73-8
9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

: 140679-78-3
9-(3-deoxy-5-O-(4-methoxytrityl)-β-D-threo-pentofuranosyl)-N¹-methylhypoxanthine

Guidance literature:: With potassium hydroxide; sodium tetrahydroborate; In methanol; benzene; for 20h; Ambient temperature;
DOI:10.1039/P19920000469

Reference yield:

: 69659-63-8
5'-O-(4-methoxytrityl)inosine

: 140679-73-8
9-{(2R,3S,5S)-3-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-1,9-dihydro-purin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1) pyridine / 1) RT, 70 min, 2) 4h, RT

2: 89 percent / KOH, NaBH₄ / methanol; benzene / 27.5 h / Ambient temperature

With pyridine; potassium hydroxide; sodium tetrahydroborate; In methanol; benzene;
DOI:10.1039/P19920000469