Technology Process of C31H30ClN7O7S
There total 6 articles about C31H30ClN7O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H21ClN6O5S;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at 0 ℃;
benzyl chloroformate;
With
sodium carbonate;
In
tetrahydrofuran; water;
Further stages.;
DOI:10.1016/j.bmcl.2007.05.090
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaN3 / dimethylformamide / 60 °C
2.1: PPh3; H2O / tetrahydrofuran / 50 °C
3.1: Et3N / CH2Cl2 / 0 °C
4.1: LiHMDS / tetrahydrofuran / 0 °C
4.2: Na2CO3 / tetrahydrofuran; H2O
With
sodium azide; water; triethylamine; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.05.090
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: PPh3; H2O / tetrahydrofuran / 50 °C
2.1: Et3N / CH2Cl2 / 0 °C
3.1: LiHMDS / tetrahydrofuran / 0 °C
3.2: Na2CO3 / tetrahydrofuran; H2O
With
water; triethylamine; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2007.05.090