C₆₂H₉₆O₁₄Si₂

Base Information

Chemical Name:C₆₂H₉₆O₁₄Si₂
CAS No.:887927-20-0
Molecular Formula:C₆₂H₉₆O₁₄Si₂
Molecular Weight:1121.61
Hs Code.:

C<sub>62</sub>H<sub>96</sub>O<sub>14</sub>Si<sub>2</sub>

Synonyms:C₆₂H₉₆O₁₄Si₂

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Chemical Property of C₆₂H₉₆O₁₄Si₂

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Technology Process of C₆₂H₉₆O₁₄Si₂

There total 7 articles about C₆₂H₉₆O₁₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 887927-17-5
(S)-3-(tert-Butyl-diphenyl-silanyloxy)-4-[(2S,6R)-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-tetrahydro-pyran-2-yl]-butan-1-ol

: 887927-20-0
C₆₂H₉₆O₁₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / phosphate buffer; NaOCl; sodium chlorite / TEMPO / acetonitrile; H₂O / 4 h / 45 °C / pH 7

2: triethylamine / toluene / 5 h / 23 - 25 °C

3: 8.5 mg / 4-(dimethylamino)pyridine / toluene / 1 h / 23 - 25 °C

With dmap; sodium hypochlorite; sodium chlorite; phosphate buffer; triethylamine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In water; toluene; acetonitrile; 3: Yamaguchi esterification;
DOI:10.1021/ol060457z

Reference yield:

: 887927-14-2
[(S)-1-((2S,6R)-6-Allyl-tetrahydro-pyran-2-ylmethyl)-3-benzyloxy-propoxy]-tert-butyl-diphenyl-silane

: 887927-20-0
C₆₂H₉₆O₁₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / K₂OsO₂(OH)4; (DHQD)2PYR; potassium carbonate / K₃Fe(CN)6 / 2-methyl-propan-2-ol; H₂O / 42 h / 4 °C

2: 86 percent / PPTS / dimethylformamide / 2.5 h / 23 - 25 °C

3: 81 percent / hydrogen / Pd(OH)2 / ethyl acetate / 18 h / 23 - 25 °C / 9308.66 Torr

4: 97 percent / phosphate buffer; NaOCl; sodium chlorite / TEMPO / acetonitrile; H₂O / 4 h / 45 °C / pH 7

5: triethylamine / toluene / 5 h / 23 - 25 °C

6: 8.5 mg / 4-(dimethylamino)pyridine / toluene / 1 h / 23 - 25 °C

With dmap; sodium hypochlorite; sodium chlorite; phosphate buffer; hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; potassium dioxotetrahydroxoosmate(VI); hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; palladium dihydroxide; potassium hexacyanoferrate(III); In water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 6: Yamaguchi esterification;
DOI:10.1021/ol060457z

Reference yield:

: 3-{(2R,6S)-6-[(S)-4-Benzyloxy-2-(tert-butyl-diphenyl-silanyloxy)-butyl]-tetrahydro-pyran-2-yl}-propane-1,2-diol

: 887927-20-0
C₆₂H₉₆O₁₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / PPTS / dimethylformamide / 2.5 h / 23 - 25 °C

2: 81 percent / hydrogen / Pd(OH)2 / ethyl acetate / 18 h / 23 - 25 °C / 9308.66 Torr

3: 97 percent / phosphate buffer; NaOCl; sodium chlorite / TEMPO / acetonitrile; H₂O / 4 h / 45 °C / pH 7

4: triethylamine / toluene / 5 h / 23 - 25 °C

5: 8.5 mg / 4-(dimethylamino)pyridine / toluene / 1 h / 23 - 25 °C

With dmap; sodium hypochlorite; sodium chlorite; phosphate buffer; hydrogen; pyridinium p-toluenesulfonate; triethylamine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; palladium dihydroxide; In water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 5: Yamaguchi esterification;
DOI:10.1021/ol060457z