Technology Process of 7-decyl-3,2',3',6'-tetrahydroxyflavone
There total 5 articles about 7-decyl-3,2',3',6'-tetrahydroxyflavone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
7-decyl-3,2',3',6'-tetramethoxyflavone;
With
boron tribromide;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
With
methanol;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
Reflux;
DOI:10.1139/v11-087
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere; Reflux
With
trimethylsilyl trifluoromethanesulfonate; boron tribromide;
In
dichloromethane;
DOI:10.1139/v11-087
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: 1.08 h / -78 - 20 °C / Inert atmosphere
1.3: 20 °C / Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.1: boron tribromide / dichloromethane / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere; Reflux
With
trimethylsilyl trifluoromethanesulfonate; boron tribromide; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1139/v11-087
