L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI)

Base Information

Chemical Name:L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI)
CAS No.:163659-44-7
Molecular Formula:C₃₃H₄₀N₂O₆
Molecular Weight:560.69
Hs Code.:
Mol file:163659-44-7.mol

Synonyms:L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI)

Chemical Property:

Boiling Point:707.9±60.0 °C(Predicted)
PKA:13?+-.0.46(Predicted)
Density:1.147±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI)

There total 2 articles about L-Phenylalanine, N-[N-[1-[[4-(1,1-dimethylethoxy)phenyl]methyl]-2-methoxy-2-oxoethyl]-D-alanyl]-, phenylmethyl ester, (R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 52616-82-7
O-tert-butyl-L-tyrosine methyl ester

: 148080-97-1
(S,S)-2-bromopropanoyl-Phe-OBzl

: 148080-99-3,163659-44-7
(S)-2-{(S)-2-[(S)-2-(4-tert-Butoxy-phenyl)-1-methoxycarbonyl-ethylamino]-propionylamino}-3-phenyl-propionic acid benzyl ester

Guidance literature:: With silver(l) oxide; In toluene; for 3h; Ambient temperature;
DOI:10.1039/c39930000304

Reference yield:

: 962-39-0
L-Phenylalanine benzyl ester

: 148080-99-3,163659-44-7
(S)-2-{(S)-2-[(S)-2-(4-tert-Butoxy-phenyl)-1-methoxycarbonyl-ethylamino]-propionylamino}-3-phenyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 75 percent / Ag₂O / toluene / 3 h / Ambient temperature

With silver(l) oxide; In toluene;
DOI:10.1039/c39930000304