(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

Base Information

Chemical Name:(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide
CAS No.:135459-19-7
Molecular Formula:C₂₀H₂₅N₅O₂S
Molecular Weight:399.517
Hs Code.:

Synonyms:(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

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Chemical Property of (S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

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Technology Process of (S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

There total 9 articles about (S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135459-17-5
(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazol-2-ylsulfanylmethyl)-phenyl]-amide

: 135459-19-7
(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; at -5 ℃; for 0.5h;
DOI:10.1016/0223-5234(91)90024-H

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 135459-19-7
(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 7 steps

1: 82.4 percent / K₂CO₃ / CHCl₃ / 1.) 4 h, 2.) RT, overnight

2: SOCl₂ / benzene / 1 h / Heating

3: NaOH / H₂O; ethanol / 2 h / Ambient temperature

4: 84.4 percent / 30percent HBr-AcOH / 3 h / Ambient temperature

5: NaHCO₃ / hexamethylphosphoric acid triamide; acetonitrile / 3 h / Ambient temperature

6: 30percent HBr-AcOH / 2.5 h / Ambient temperature

7: m-chloroperbenzoic acid / CH₂Cl₂; methanol / 0.5 h / -5 °C

With sodium hydroxide; thionyl chloride; hydrogen bromide; sodium hydrogencarbonate; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; water; acetonitrile; benzene;
DOI:10.1016/0223-5234(91)90024-H

Reference yield:

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 135459-19-7
(S)-2,6-Diamino-hexanoic acid [2-(1H-benzoimidazole-2-sulfinylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / hexamethylphosphoric acid triamide; acetonitrile / 0.25 h / -5 °C

2: NaHCO₃ / hexamethylphosphoric acid triamide; acetonitrile / 3 h / Ambient temperature

3: 30percent HBr-AcOH / 2.5 h / Ambient temperature

4: m-chloroperbenzoic acid / CH₂Cl₂; methanol / 0.5 h / -5 °C

With thionyl chloride; hydrogen bromide; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; acetonitrile;
DOI:10.1016/0223-5234(91)90024-H