{dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

Base Information

Chemical Name:{dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate
CAS No.:112947-39-4
Molecular Formula:C₆₆H₇₄N₂O₁₀P₈Rh₂*2ClO₄
Molecular Weight:1707.82
Hs Code.:

Synonyms:{dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

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Chemical Property of {dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

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Technology Process of {dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

There total 1 articles about {dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 112947-57-6
{dirhodium(I)(cycloocta-1,5-diene)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

: 34244-05-8
methylbis(dimethoxyphosphino)amine

: 112947-39-4
{dirhodium(I)(methylbis(dimethoxyphosphino)amine)2(μ-2,5-bis(diphenylphosphino)furan)2} diperchlorate

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

Guidance literature:: With CO; In dichloromethane; passage of CO through the CH2Cl2 soln. of the Rh compd. to remove COD and dropwise addn. of 2 equiv. of the phosphine under N2; evapn. (vac.), washing with diethyl ether, dissolving the yellow powder in acetone, filtn. and diln. with diethyl ether;
DOI:10.1021/om00094a031