1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

Base Information

Chemical Name:1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide
CAS No.:117138-53-1
Molecular Formula:C₁₉H₁₆N₂O₂
Molecular Weight:304.348
Hs Code.:

1-benzoyl-1,2,2a,3-tetrahydrobenz<cd>indole-5-carboxamide

Synonyms:1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

Chemical Property:

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Technology Process of 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

There total 3 articles about 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 117138-52-0
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

: 117138-53-1
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

Guidance literature:: With sulfuric acid; at 90 ℃; for 2.2h;
DOI:10.1248/cpb.35.4793

Reference yield:

: 132008-45-8,51867-02-8
1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

: 117138-53-1
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: LiCN / tetrahydrofuran / 0.5 h / Ambient temperature

2: 90 percent / BF₃*Et₂O / benzene / 1.5 h / Ambient temperature

3: 100 percent / 77percent H₂SO₄ / 2.2 h / 90 °C

With sulfuric acid; boron trifluoride diethyl etherate; lithium cyanide; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.35.4793

Reference yield:

: 117138-51-9
Phosphoric acid 1-benzoyl-5-cyano-1,2,2a,3,4,5-hexahydro-benzo[cd]indol-5-yl ester diethyl ester

: 117138-53-1
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / BF₃*Et₂O / benzene / 1.5 h / Ambient temperature

2: 100 percent / 77percent H₂SO₄ / 2.2 h / 90 °C

With sulfuric acid; boron trifluoride diethyl etherate; In benzene;
DOI:10.1248/cpb.35.4793