Technology Process of C19H23NO2
There total 2 articles about C19H23NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1S,4S)-2,5-diphenylbicyclo[2.2.2]octa-2,5-diene; chlorobis(ethylene)rhodium(I) dimer;
In
1,4-dioxane;
at 25 ℃;
for 1h;
Overall yield = 92 %; enantioselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c2cc36961c
DOI:10.1039/c2cc36961c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Schlenk technique; Inert atmosphere
2: chlorobis(ethylene)rhodium(I) dimer; (1S,4S)-2,5-diphenylbicyclo[2.2.2]octa-2,5-diene / 1,4-dioxane / 1 h / 25 °C / Schlenk technique; Inert atmosphere
With
(1S,4S)-2,5-diphenylbicyclo[2.2.2]octa-2,5-diene; chlorobis(ethylene)rhodium(I) dimer; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
1,4-dioxane; dichloromethane;
DOI:10.1039/c2cc36961c
DOI:10.1039/c2cc36961c