ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Base Information

Chemical Name:ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate
CAS No.:959939-28-7
Molecular Formula:C₁₇H₂₁FN₄O₇
Molecular Weight:412.375
Hs Code.:

Synonyms:ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Suppliers and Price of ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

There total 4 articles about ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 959939-27-6
ethyl cis-4-[2-fluoro-3-[(methoxycarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

: 959939-28-7
ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: With hydrazine; In ethanol; at 20 ℃; for 1h;

Reference yield:

: 211693-73-1
2-amino-3,4-difluoronitro-benzene

: 959939-28-7
ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / 1,4-dioxane; water / 18 h / 100 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 72 h / 10 - 20 °C

3: pyridine / dichloromethane / 0.5 h / 10 °C

4: hydrazine / ethanol / 1 h / 20 °C

With pyridine; potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; triphenylphosphine; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;

Reference yield:

: 959939-24-3
3-amino-2-fluoro-4-nitrophenol

: 959939-28-7
ethyl cis-4-[2-fluoro-3-[(hydrazinecarbonylformyl)amino]-4-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 72 h / 10 - 20 °C

2: pyridine / dichloromethane / 0.5 h / 10 °C

3: hydrazine / ethanol / 1 h / 20 °C

With pyridine; triphenylphosphine; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;