3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

Base Information

Chemical Name:3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester
CAS No.:872255-76-0
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

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Chemical Property of 3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

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Technology Process of 3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

There total 2 articles about 3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 307989-15-7
3-(4-formylbenzoylamino)propionic acid methyl ester

: 86560-47-6
(3,3-dimethylbutyl)-magnesium bromide

: 872255-76-0
3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

Guidance literature:: 3-(4-formylbenzoylamino)propionic acid methyl ester; (3,3-dimethylbutyl)-magnesium bromide; In tetrahydrofuran; at 0 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 872255-76-0
3-[4-(1-hydroxy-4,4-dimethyl-pentyl)-benzoylamino]-propionic methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine / dichloromethane / 20 °C

1.2: 20 °C

2.1: tetrahydrofuran / 1 h / 0 °C

2.2: 0 °C

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In tetrahydrofuran; dichloromethane;