Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI)

Base Information

• Chemical Name: Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI)
• CAS No.: 163332-93-2
• Molecular Formula: C₁₀H₈
• Molecular Weight: 128.174
• Mol file: 163332-93-2.mol

Synonyms:Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI)

Chemical Property of Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI)

Chemical Property:

• Boiling Point: 156.7±7.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.43±0.1 g/cm3(Predicted)
• LogP: 0.98740

Purity/Quality:

1-ethynylcubane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI)

There total 1 articles about Pentacyclo[4.2.0.02,5.03,8.04,7]octane, ethynyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,2-dibromovinyl)cubane (163332-90-9) → ethynylcubane (163332-93-2)

Guidance literature:

With hydrogenchloride; n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, RT;

DOI:10.1021/ja00096a016

Reference yield:

ethynylcubane (163332-93-2) → 1-ethynyltricyclooctadiene (163333-05-9)

Guidance literature:

With di-μ-chlorobis(norbornadiene)dirhodium(I); In chloroform; for 3h; Ambient temperature;

DOI:10.1021/ja00096a016

upstream raw materials:

(2,2-dibromovinyl)cubane

Downstream raw materials:

1-ethynyltricyclooctadiene

Refernces