C₄₈H₃₆N₂

Base Information

Chemical Name:C₄₈H₃₆N₂
CAS No.:1413338-15-4
Molecular Formula:C₄₈H₃₆N₂
Molecular Weight:640.827
Hs Code.:

C<sub>48</sub>H<sub>36</sub>N<sub>2</sub>

Synonyms:C₄₈H₃₆N₂

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Chemical Property of C₄₈H₃₆N₂

Chemical Property:

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Technology Process of C₄₈H₃₆N₂

There total 12 articles about C₄₈H₃₆N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1413338-08-5
C₅₇H₅₆N₂Si

: 1413338-15-4
C₄₈H₃₆N₂

Guidance literature:: With tetrabutyl ammonium fluoride; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ja309393c

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1413338-15-4
C₄₈H₃₆N₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: trichlorophosphate / 2 h / 45 - 50 °C

2.1: sodium tetrahydroborate / dichloromethane; methanol / 2 h / 20 °C

3.1: phosphorus tribromide / diethyl ether / 15 h / 0 - 20 °C

4.1: toluene / 24 h / Reflux

5.1: potassium tert-butylate / tetrahydrofuran / 3.67 h / Inert atmosphere; Reflux

5.2: 15 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol; water / 15 h / 20 °C

7.1: phosphorus tribromide / tetrahydrofuran; diethyl ether / 15 h / 0 - 20 °C

8.1: toluene / 16 h / Reflux

9.1: potassium tert-butylate / tetrahydrofuran / 3 h / Reflux

10.1: tetrabutyl ammonium fluoride / 15 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; potassium tert-butylate; tetrabutyl ammonium fluoride; phosphorus tribromide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; 9.1: |Wittig Olefination;
DOI:10.1021/ja309393c

Reference yield:

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 1413338-15-4
C₄₈H₃₆N₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide; acetic acid / chloroform; acetone / 15 h / 0 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / Inert atmosphere

2.2: 24 h / Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 3 h / Reflux

4.1: tetrabutyl ammonium fluoride / 15 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; potassium tert-butylate; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; chloroform; acetone; 3.1: |Wittig Olefination;
DOI:10.1021/ja309393c