Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

Base Information

Chemical Name:Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester
CAS No.:201009-39-4
Molecular Formula:C₂₀H₁₇F₅O₄
Molecular Weight:416.345
Hs Code.:

Synonyms:Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

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Chemical Property of Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

Chemical Property:

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Technology Process of Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

There total 1 articles about Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: Deca-2,8-diynedioic acid mono-tert-butyl ester

: 201009-39-4
Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -20 - 20 ℃;
DOI:10.1039/a704927g

Reference yield:

: 201009-39-4
Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

: (2E,4E)-Deca-2,4-dien-8-ynedioic acid 10-tert-butyl ester 1-pentafluorophenyl ester

Guidance literature:: With triphenylphosphine; In toluene; at 50 ℃; for 5h;
DOI:10.1039/a704927g

Reference yield:

: 201009-39-4
Deca-2,8-diynedioic acid tert-butyl ester pentafluorophenyl ester

: (6E,8E)-9-((S)-1-Carbamoyl-2-phenyl-ethylcarbamoyl)-nona-6,8-dien-2-ynoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃ / toluene / 5 h / 50 °C

2: toluene / 14 h / Ambient temperature

With triphenylphosphine; In toluene;
DOI:10.1039/a704927g