Technology Process of C34H54N2
There total 5 articles about C34H54N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol / 20 °C / Molecular sieve
2: sodium tetrahydroborate / methanol / 0 - 20 °C
With
sodium tetrahydroborate;
In
methanol;
DOI:10.1016/j.bmcl.2012.12.083
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis(triphenylphosphine)palladium(II) dichloride; triethylamine; copper(l) iodide / tetrahydrofuran / 12 h / 50 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C
3: methanol / 20 °C / Molecular sieve
4: sodium tetrahydroborate / methanol / 0 - 20 °C
With
sodium tetrahydroborate; copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; ethyl acetate;
1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2012.12.083