C₁₉H₁₇N₃O₃

Base Information

• Chemical Name: C₁₉H₁₇N₃O₃
• CAS No.: 1315476-14-2
• Molecular Formula: C₁₉H₁₇N₃O₃
• Molecular Weight: 335.362
• Mol file: 1315476-14-2.mol

Synonyms:C₁₉H₁₇N₃O₃

Chemical Property of C₁₉H₁₇N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₉H₁₇N₃O₃

There total 1 articles about C₁₉H₁₇N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitroveratraldehyde (55149-84-3) → C19H17N3O3 (1315476-14-2)

Guidance literature:

Multi-step reaction with 12 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 1.25 h / -2 °C

2.1: palladium on carbon; formic acid; ammonium formate / methanol / 1 h

3.1: 2 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / Reflux

5.1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 9 h

6.1: potassium tert-butylate / tetrahydrofuran / 6 h / 0 °C

7.1: 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene / water / 1 h / 0 °C

8.1: hydrogenchloride / methanol / 0.5 h / 20 °C / Inert atmosphere

8.2: 16 h / 20 °C / Inert atmosphere

9.1: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 0.5 h / 20 °C / Inert atmosphere

10.1: boron trifluoride diethyl etherate / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

11.1: hydrogen bromide; acetic acid / dichloromethane / 36 h / 0 - 20 °C / Inert atmosphere

12.1: sodium methylate / tetrahydrofuran; methanol / 0.5 h / 0 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; formic acid; 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on carbon; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen bromide; ammonium formate; sodium methylate; acetic acid; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; potassium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; toluene; 5.1: Mitsunobu reaction;

DOI:10.1039/c1ob05058c

upstream raw materials:

2-nitroveratraldehyde