tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

Base Information

Chemical Name:tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate
CAS No.:1384878-46-9
Molecular Formula:C₃₅H₃₉F₃N₄O₆
Molecular Weight:668.713
Hs Code.:

Synonyms:tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

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Chemical Property of tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

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Technology Process of tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

There total 7 articles about tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1384878-45-8
C₃₀H₃₁F₃N₄O₄

: 1384878-46-9
tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 852814-99-4
ethyl 4-[4-(1-methylethyl)phenyl]-2,4-dioxobutanoate

: 1384878-46-9
tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / ethanol / 0.25 h / 20 °C

1.2: Reflux

2.1: triethylamine / dmap / tert-butyl alcohol / 16 h / 60 °C

3.1: trichloroisocyanuric acid / 1,1-dichloroethane / 16 h / Reflux

4.1: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C

5.1: trimethylphosphane / tetrahydrofuran / 3 h / 20 °C

6.1: triethylamine / dichloromethane / 1 h / 20 °C

With sodium azide; trichloroisocyanuric acid; triethylamine; trimethylphosphane; dmap; acetic acid; In tetrahydrofuran; 1,1-dichloroethane; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1260597-59-8
3-hydroxy-4-(4-isopropyl-benzoyl)-1-(6-methyl-pyridazin-3-yl)-5-(4-trifluoromethoxy-phenyl)-1,5-dihydro-pyrrol-2-one

: 1384878-46-9
tert-butyl N-[[6-[4-tert-butoxy-3-(4-isopropylbenzoyl)-5-oxo-2-[4-(trifluoromethoxy)phenyl]-2H-pyrrol-1-yl]pyridazin-3-yl]methyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dmap / tert-butyl alcohol / 16 h / 60 °C

2: trichloroisocyanuric acid / 1,1-dichloroethane / 16 h / Reflux

3: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C

4: trimethylphosphane / tetrahydrofuran / 3 h / 20 °C

5: triethylamine / dichloromethane / 1 h / 20 °C

With sodium azide; trichloroisocyanuric acid; triethylamine; trimethylphosphane; dmap; In tetrahydrofuran; 1,1-dichloroethane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;