(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

Base Information

Chemical Name:(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide
CAS No.:1127304-33-9
Molecular Formula:C₃₆H₄₄F₁₇NO₆SSi
Molecular Weight:969.873
Hs Code.:

(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

Synonyms:(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

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Chemical Property of (Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

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Technology Process of (Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

There total 1 articles about (Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1127305-21-8
(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-acetoxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

: 1127304-33-9
(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

Guidance literature:: With methanol; ammonia; at 20 ℃; for 44h; Inert atmosphere;
DOI:10.1002/anie.200804486

Reference yield: 16.0%

: 1034352-90-3
(4-(allyloxy)but-2-ynyloxy)diisopropylsilane

: 1127304-33-9
(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

: 1127305-41-2
(1''S,4''R)-N-[2-((Z)-4'-{[4''-(4'''-{allyloxy}but-2'''-ynyloxy-diisopropyl-silanyloxy)-cyclopent-2''-enyloxy]-diisopropyl-silanyloxy}-but-2''-enyloxymethyl)-allyl]-N-(3'''',3'''',4'''',4'''',5'''',5'''',6'''',6'''',7'''',7'''',8'''',8'''',9'''',9'''',10'''',10'''',10''''-heptadecafluorodecyl)-4'''''-methyl-benzenesulfonamide

Guidance literature:: (4-(allyloxy)but-2-ynyloxy)diisopropylsilane; With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide; With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200804486

Reference yield: 16.0%

: 1127304-33-9
(Z)-(1'''S,4'''R)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-(2'-{4''-[(4'''-hydroxycyclopent-2'''-en-1'''-yloxy)diisopropylsilanyloxy]-but-2''-enyloxymethyl}-allyl)-4''''-methylbenzenesulfonamide

: 1745-81-9
o-Allylphenol

: 1127305-45-6
(1''S,4''S)-N-[2-((Z)-4'-{[4''-(2'''-allyl-phenoxy)-cyclopent-2''-enyloxy]-diisopropyl-silanyloxy}-but-2'-enyloxymethyl)-allyl]-N-(3'''',3'''',4'''',4'''',5'''',5'''',6'''',6'''',7'''',7'''',8'''',8'''',9'''',9'''',10'''',10'''',10''''-heptadecafluorodecyl)-4'''''-methyl-benzenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/anie.200804486