BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]-

Base Information

• Chemical Name: BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]-
• CAS No.: 881913-20-8
• Molecular Formula: C₁₆H₁₃BO₂
• Molecular Weight: 248.089
• Hs Code.: 2931900090
• Mol file: 881913-20-8.mol

Synonyms:(3-(naphthalen-1-yl)phenyl)boronic acid

Chemical Property of BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]-

Chemical Property:

• Boiling Point: 471.9±48.0 °C(Predicted)
• PKA: 8.27±0.19(Predicted)
• Density: 1.23±0.1 g/cm3(Predicted)
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

[3-(1-Naphthalenyl)phenyl]boronicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Boronic acid, [3-(1-naphthalenyl)phenyl]-

Technology Process of BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]-

There total 6 articles about BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-Bromonaphthalene (90-11-9) + 1,3-phenylenediboronic acid (4612-28-6) → (3-(naphthalen-1-yl)phenyl)boronic acid (881913-20-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 2h;

Reference yield: 67.0%

1-bromo-3-(1-naphthyl)benzene → (3-(naphthalen-1-yl)phenyl)boronic acid (881913-20-8)

Guidance literature:

1-bromo-3-(1-naphthyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -60 ℃; for 2h; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; hexane; at -60 - 20 ℃; for 17h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; hexane; water; at 20 ℃; for 1h;

Reference yield: 67.0%

1-bromo-3-(1-naphthyl)benzene + Triisopropyl borate (5419-55-6) → (3-(naphthalen-1-yl)phenyl)boronic acid (881913-20-8)

Guidance literature:

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane; toluene;

upstream raw materials:

Triisopropyl borate

1-Naphthylboronic acid

1-Bromo-3-iodobenzene

1-Bromonaphthalene

Downstream raw materials:

C₂₂H₁₅Br

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