α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

Base Information

Chemical Name:α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline
CAS No.:96409-42-6
Molecular Formula:C₁₉H₁₄ClN₇O₂
Molecular Weight:407.819
Hs Code.:

Synonyms:α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

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Chemical Property of α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

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Technology Process of α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

There total 6 articles about α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 89-98-5
2-chloro-benzaldehyde

: 96409-39-1
syn-3-(α-Hydroxyimino-4-amino-5-methyl-4H-1,2,4-triazol-3-ylmethyl)-2-oxo-1,2-dihydroquinoxaline

: 96409-42-6
3-<α-Hydroxyimino-4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

Guidance literature:: In N,N-dimethyl-formamide; for 3h; Heating;
DOI:10.1002/jhet.5570220649

Reference yield: 75.5%

: 89-98-5
2-chloro-benzaldehyde

: 96409-40-4
3-(α-Hydroxyimino-5-methyl-2H-1,2,4-triazol-3-ylmethyl)-2-oxo-1,2-dihydroquinoxaline

: 96409-42-6
α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

Guidance literature:

Reference yield:

: 85936-45-4
[3-Oxo-3,4-dihydro-1H-quinoxalin-(2Z)-ylidene]-acetic acid [1-ethoxy-eth-(Z)-ylidene]-hydrazide

: 96409-42-6
α-hydroxyimino-3-<4-(o-chlorobenzylideneamino)-5-methyl-4H-1,2,4-triazol-3-ylmethyl>-2-oxo-1,2-dihydroquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: 80.3 percent / NH₂NH₂*H₂O, 1,8-diazabicyclo<5,4,0>-7-undecene (DBU) / ethanol

2: 97.4 percent / NaNO₂, AcOH / H₂O

3: 75.5 percent

With hydrazine hydrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium nitrite; In ethanol; water;