1-(2,4-dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one

Base Information

• Chemical Name: 1-(2,4-dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one
• CAS No.: 56944-69-5
• Molecular Formula: C₁₁H₁₀Cl₂OS₂
• Molecular Weight: 293.238
• Mol file: 56944-69-5.mol

Synonyms:3,3-Bis-methylthio-1-(2',4'-dichlorphenyl)-2-propen-1-on

Chemical Property of 1-(2,4-dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1-(2,4-Dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one ^*data from reagent suppliers

Safty Information:

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Technology Process of 1-(2,4-dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one

There total 1 articles about 1-(2,4-dichlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,3-Bis-methylthio-1-(2',4'-dichlorphenyl)-2-propen-1-on (56944-69-5)

Guidance literature:

II (R=2,4-Cl2), MeI/NaOMe;

Reference yield: 93.0%

3,3-Bis-methylthio-1-(2',4'-dichlorphenyl)-2-propen-1-on (56944-69-5) → 2-bromo-1-(2,4-dichlorophenyl)-3,3-bis(methylthio)prop-2-en-1-one

Guidance literature:

With Oxone; potassium bromide; In water; acetonitrile; at 20 ℃;

DOI:10.1039/d0nj03737k

Reference yield: 82.0%

3,3-Bis-methylthio-1-(2',4'-dichlorphenyl)-2-propen-1-on (56944-69-5) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 3-(2,4-dichlorobenzoyl)-2H-benzo[f]chromen-2-one

Guidance literature:

With piperidine; In ethanol; Reflux;

DOI:10.1134/S1068162017020054

Downstream raw materials:

3-(2,4-dichlorophenyl)-5-methylthio-isoxazole

5-(2,4-Dichloro-phenyl)-3-methylsulfanyl-isoxazole

1-(2,4-dichlorophenyl)-2-(imidazolidin-2-ylidene)ethanone

1-(2,4-dichlorophenyl)-2-(tetrahydropyrimidin-2(1H)-ylidene)ethanone

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