4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

Base Information

Chemical Name:4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate
CAS No.:1422423-75-3
Molecular Formula:C₃₁H₃₄BrN₃O₃
Molecular Weight:576.533
Hs Code.:

Synonyms:4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

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Chemical Property of 4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

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Technology Process of 4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

There total 5 articles about 4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1422423-68-4
C₉H₅BrClN₃O

: 91577-95-6
4-hydroxy-4'-decyloxybiphenyl

: 1422423-75-3
4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; for 48h; Reflux; Cooling with ice; Inert atmosphere;
DOI:10.1016/j.molstruc.2012.09.020

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 1422423-75-3
4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / 24 h

2: triethylamine / dichloromethane / 48 h / Reflux; Cooling with ice; Inert atmosphere

With triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.molstruc.2012.09.020

Reference yield:

: 112-29-8
1-bromo dodecane

: 1422423-75-3
4-(decyloxy)biphenyl 1-(4-bromophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / 24 h

2: triethylamine / dichloromethane / 48 h / Reflux; Cooling with ice; Inert atmosphere

With triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.molstruc.2012.09.020