C₆₉H₆₂O₆

Base Information

• Chemical Name: C₆₉H₆₂O₆
• CAS No.: 1313187-42-6
• Molecular Formula: C₆₉H₆₂O₆
• Molecular Weight: 987.248
• Mol file: 1313187-42-6.mol

Synonyms:C₆₉H₆₂O₆

Chemical Property of C₆₉H₆₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₉H₆₂O₆

There total 3 articles about C₆₉H₆₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C22H15BrO3 (1313187-41-5) + 9,9-dihexyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)fluorene (254755-24-3) → C69H62O6 (1313187-42-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 70 ℃; Inert atmosphere;

DOI:10.1002/anie.201007277

Reference yield:

2,7-dibromofluorene-9-one (14348-75-5) → C69H62O6 (1313187-42-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 70 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 70 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; In tetrahydrofuran; water;

DOI:10.1002/anie.201007277

Reference yield:

p-ethoxycarbonylphenylboronic acid (4334-88-7) → C69H62O6 (1313187-42-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 70 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 70 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; In tetrahydrofuran; water;

DOI:10.1002/anie.201007277

upstream raw materials:

C₂₂H₁₅BrO₃

9,9-dihexyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)fluorene

2,7-dibromofluorene-9-one

p-ethoxycarbonylphenylboronic acid

Downstream raw materials:

(HOOCC₆H₄C₁₃H₆O)2C₁₃H₆(C₆H₁₃)2

Refernces