C₃₈H₄₃NO₉

Base Information

• Chemical Name: C₃₈H₄₃NO₉
• CAS No.: 1383446-36-3
• Molecular Formula: C₃₈H₄₃NO₉
• Molecular Weight: 657.761
• Mol file: 1383446-36-3.mol

Synonyms:C₃₈H₄₃NO₉

Chemical Property of C₃₈H₄₃NO₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₄₃NO₉

There total 6 articles about C₃₈H₄₃NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H37NO7 + benzyl chloroformate (501-53-1,94274-21-2) → C38H43NO9 (1383446-36-3)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 0 - 20 ℃; for 12h;

DOI:10.1016/j.carres.2012.04.010

Reference yield:

C30H33N3O7 (1383446-34-1) → C38H43NO9 (1383446-36-3)

Guidance literature:

Multi-step reaction with 3 steps

1: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 10 h / -78 °C

2: tributylphosphine / dichloromethane / 20 °C

3: sodium hydrogencarbonate / tetrahydrofuran; water / 12 h / 0 - 20 °C

With tributylphosphine; di-n-butylboryl trifluoromethanesulfonate; borane; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/j.carres.2012.04.010

Reference yield:

(2R,3R,4S,5S,6R)-2-(2-Azido-ethoxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol (165331-08-8) → C38H43NO9 (1383446-36-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 10-camphorsufonic acid / tetrahydrofuran / 10 h / Reflux

2: sodium hydride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

3: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 10 h / -78 °C

4: tributylphosphine / dichloromethane / 20 °C

5: sodium hydrogencarbonate / tetrahydrofuran; water / 12 h / 0 - 20 °C

With tributylphosphine; di-n-butylboryl trifluoromethanesulfonate; 10-camphorsufonic acid; borane; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.carres.2012.04.010

upstream raw materials:

benzyl chloroformate

C₃₀H₃₃N₃O₇

2'-azidoethyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-β-D-glucopyranoside

2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Downstream raw materials:

C₇₃H₉₀N₄O₁₄Si₂