2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

Base Information

• Chemical Name: 2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate
• CAS No.: 65472-78-8
• Molecular Formula: C₄H₄O₄*C₃₀H₃₆N₂O₃
• Molecular Weight: 588.701

Synonyms:2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

Chemical Property of 2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

There total 8 articles about 2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.9%

(2E)-but-2-enedioic acid (110-17-8,26099-09-2) + 2-(4-benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-3,4-dihydro-2H-naphthalen-1-one (65472-73-3) → (1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid (65472-78-8,88284-69-9,88284-71-3) + (1R,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid (65472-78-8,88284-69-9,88284-71-3)

Guidance literature:

With sodium tetrahydroborate; In methanol; chloroform; for 0.5h; Ambient temperature;

DOI:10.1248/cpb.31.2006

Reference yield: 8.9%

(2E)-but-2-enedioic acid (110-17-8,26099-09-2) + 2-(4-benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-3,4-dihydro-2H-naphthalen-1-one (65472-73-3) → (1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid (65472-78-8,88284-69-9,88284-71-3) + (1R,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid (65472-78-8,88284-69-9,88284-71-3)

Guidance literature:

With sodium tetrahydroborate; In methanol; chloroform; for 0.5h; Ambient temperature;

DOI:10.1248/cpb.31.2006

Reference yield:

(2E)-but-2-enedioic acid (110-17-8,26099-09-2) + 2-(4-benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-3,4-dihydro-2H-naphthalen-1-one (65472-73-3) → 2-(4-benzhydryl-1-piperazinylmethyl)-5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate (65472-78-8)

Guidance literature:

With sodium borohydrid; In methanol; diethyl ether; chloroform; water;

upstream raw materials:

(2E)-but-2-enedioic acid

2-(4-benzhydryl-piperazin-1-ylmethyl)-5,6-dimethoxy-3,4-dihydro-2H-naphthalen-1-one

5,6-dimethoxy-1-tetralone

N-benzhydrylpiperazine hydrochloride

Downstream raw materials:

1-Benzhydryl-4-(5,6-dimethoxy-3,4-dihydro-naphthalen-2-ylmethyl)-piperazine; hydrochloride

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