D-Glucose, 2,3,4,5,6-penta-O-methyl-, cyclic (R)-1,1-binaphthalene-2,2-diyl dithioacetal

Base Information

Chemical Name:D-Glucose, 2,3,4,5,6-penta-O-methyl-, cyclic (R)-1,1-binaphthalene-2,2-diyl dithioacetal
CAS No.:162825-40-3
Molecular Formula:C₃₁H₃₄O₅S₂
Molecular Weight:550.74
Hs Code.:

Synonyms:D-Glucose,2,3,4,5,6-penta-O-methyl-, cyclic [1,1'-binaphthalene]-2,2'-diyl mercaptal,(R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-Glucose, 2,3,4,5,6-penta-O-methyl-, cyclic (R)-1,1-binaphthalene-2,2-diyl dithioacetal

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of D-Glucose, 2,3,4,5,6-penta-O-methyl-, cyclic (R)-1,1-binaphthalene-2,2-diyl dithioacetal

There total 2 articles about D-Glucose, 2,3,4,5,6-penta-O-methyl-, cyclic (R)-1,1-binaphthalene-2,2-diyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102555-71-5,124414-36-4,124414-37-5
1,1'-binaphthalene-2,2'-dithiol

: 2,3,4,5,6-penta-O-methyl-D-glucose diethylthioacetal

: 162825-40-3,162825-41-4
(S)-4<(1''R,2''S,3''R,4''R)-1'',2'',3'',4'',5''-pentamethoxypentyl>-dinaphtho<2,1-d:1',2'-f><1,3>dithipin

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -15 - 15 ℃;
DOI:10.1016/0957-4166(94)00387-Q

Reference yield:

: 102555-71-5,124414-36-4,124414-37-5
1,1'-binaphthalene-2,2'-dithiol

: 2,3,4,5,6-penta-O-methyl-D-glucose

: 162825-40-3,162825-41-4
(S)-4<(1''R,2''S,3''R,4''R)-1'',2'',3'',4'',5''-pentamethoxypentyl>-dinaphtho<2,1-d:1',2'-f><1,3>dithipin

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; Ambient temperature;
DOI:10.1016/0957-4166(94)00387-Q

Reference yield:

: 162825-40-3,162825-41-4
(S)-4<(1''R,2''S,3''R,4''R)-1'',2'',3'',4'',5''-pentamethoxypentyl>-dinaphtho<2,1-d:1',2'-f><1,3>dithipin

: 188-57-8,79252-43-0,79252-44-1
(R)-(-)-dinaphtho<2,1-c:1',2'-e><1,2>dithiin

Guidance literature:: With boron trifluoride diethyl etherate; iron(III) chloride; ethane-1,2-dithiol; Yield given. Multistep reaction; 1.) CH₂Cl₂, RT, 12 h, 2.) EtOH, reflux, 30 min;
DOI:10.1016/0957-4166(94)00387-Q