(2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3

Base Information

Chemical Name:(2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3
CAS No.:256957-41-2
Molecular Formula:C₃₇H₅₃NO₂Ti
Molecular Weight:591.713
Hs Code.:

Synonyms:(2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3

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Chemical Property of (2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3

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Technology Process of (2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3

There total 1 articles about (2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 256957-38-7
(2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]Cl

: 7412-67-1
neopentyl lithium

: 256957-41-2
(2,2'-methylenebis(4-methyl)-6-tert-butylphenolate)[Ti(η(2)-C6H4(o-CH2NMe2))]CH2CMe3

Guidance literature:: In diethyl ether; N2-atmosphere; addn. of LiCH2(t)Bu to Ti-complex (-80°C), stirring for 2 h, warming to room temp., stirring for 20 min; solvent removal (vac.), stirring with pentane, evapn. (vac.), extn. intopentane, evapn., washing (pentane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(99)00504-5