2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester

Base Information

• Chemical Name: 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester
• CAS No.: 474640-41-0
• Molecular Formula: C₂₂H₂₆N₂O₆S
• Molecular Weight: 446.524

Synonyms:2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester

Chemical Property of 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester

Chemical Property:

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Technology Process of 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester

There total 3 articles about 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-benzoylamino-4-ethoxythiocarbonylsulfanyl-5-[methanesulfonyl-(4-methoxy-phenyl)-amino]-pentanoic acid ethyl ester (474640-38-5) → 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester (474640-41-0)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1039/b204371h

Reference yield:

N-(4-methoxyphenyl)-N-(prop-2-en-1-yl)methanesulfonamide (23004-83-3) → 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester (474640-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 60 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane;

DOI:10.1039/b204371h

Reference yield:

benzoylamino-ethoxythiocarbonylsulfanyl-acetic acid ethyl ester → 2-benzoylamino-3-(1-methanesulfonyl-5-methoxy-2,3-dihydro-1H-indol-3-yl)-propionic acid ethyl ester (474640-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 60 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane;

DOI:10.1039/b204371h

upstream raw materials:

2-benzoylamino-4-ethoxythiocarbonylsulfanyl-5-[methanesulfonyl-(4-methoxy-phenyl)-amino]-pentanoic acid ethyl ester

N-(4-methoxyphenyl)-N-(prop-2-en-1-yl)methanesulfonamide

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