Technology Process of phenyl 3-oxo-5-hydroxy-amyl sulfide
There total 3 articles about phenyl 3-oxo-5-hydroxy-amyl sulfide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) n-butyllithium / 1.) tetrahydrofuran/hexane, -78 deg C, then to -35 deg C, 1.5 h, 2.) -70 deg C, then 10 deg C, 2 d
2: 65 percent / mercury(II) chloride, calcium carbonate / acetonitrile; H2O / 9 h / Heating
With
n-butyllithium; calcium carbonate; mercury dichloride;
In
water; acetonitrile;
DOI:10.1016/S0040-4020(01)82341-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) triethylamine, 2.) boron trifluoride etherate / 1.) chloroform, 3 h, 12 deg C, 2.) 4 h, 12 deg C
2: 1.) n-butyllithium / 1.) tetrahydrofuran/hexane, -78 deg C, then to -35 deg C, 1.5 h, 2.) -70 deg C, then 10 deg C, 2 d
3: 65 percent / mercury(II) chloride, calcium carbonate / acetonitrile; H2O / 9 h / Heating
With
n-butyllithium; boron trifluoride diethyl etherate; triethylamine; calcium carbonate; mercury dichloride;
In
water; acetonitrile;
DOI:10.1016/S0040-4020(01)82341-3
![2-[2-(2-Phenylsulfanyl-ethyl)-[1,3]dithian-2-yl]-ethanol](/Databaselist/images/loading.webp)
