3,3-bis(but-2-enyloxy)-1-propynylbenzene

Base Information

Chemical Name:3,3-bis(but-2-enyloxy)-1-propynylbenzene
CAS No.:853661-62-8
Molecular Formula:C₁₇H₂₀O₂
Molecular Weight:256.345
Hs Code.:

Synonyms:3,3-bis(but-2-enyloxy)-1-propynylbenzene

Suppliers and Price of 3,3-bis(but-2-enyloxy)-1-propynylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,3-bis(but-2-enyloxy)-1-propynylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,3-bis(but-2-enyloxy)-1-propynylbenzene

There total 2 articles about 3,3-bis(but-2-enyloxy)-1-propynylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 853661-62-8
3,3-bis(but-2-enyloxy)-1-propynylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: PCC / CH₂Cl₂ / 3 h / 0 - 20 °C

2: 1.07 g / pTsOH / benzene / 16 h / Heating

With toluene-4-sulfonic acid; pyridinium chlorochromate; In dichloromethane; benzene;
DOI:10.1002/ejoc.200400886

Reference yield:

: 2579-22-8
Phenylpropargyl aldehyde

: 504-61-0,542-72-3
(E)-but-2-enol

: 853661-62-8
3,3-bis(but-2-enyloxy)-1-propynylbenzene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 16h; Heating;
DOI:10.1002/ejoc.200400886

Reference yield: 71.0%

: 853661-62-8
3,3-bis(but-2-enyloxy)-1-propynylbenzene

: (4SR,5SR,8RS)-8-((E)-but-2-enyloxy)-4-methyl-2-phenyl-7-oxabicyclo[3.3.0]oct-1-ene-3-one

Guidance literature:: 3,3-bis(but-2-enyloxy)-1-propynylbenzene; Co₂(CO)8; With 4 A molecular sieve; In dichloromethane; at 20 ℃; for 2h;

With air; trimethylamine-N-oxide; In dichloromethane; at -20 - 20 ℃;
DOI:10.1002/ejoc.200400886