10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

Base Information

Chemical Name:10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones
CAS No.:60878-55-9
Molecular Formula:C₂₅H₃₁N₃O
Molecular Weight:389.541
Hs Code.:

Synonyms:10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

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Chemical Property of 10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

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Technology Process of 10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

There total 3 articles about 10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 93360-41-9
10,10,10a-trimethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

: 120-21-8
4-Diethylaminobenzaldehyde

: 60878-55-9
10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

Guidance literature:: With acetic anhydride; acetic acid; at 100 ℃; for 3h;
DOI:10.1007/BF01175058

Reference yield:

: 1640-39-7
2,3,3-trimethylindoleniune

: 60878-55-9
10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / acetic acid / 2 h / 100 °C

2: 93 percent / CH₃COOH,(CH₃CO)2O / 3 h / 100 °C

With acetic anhydride; acetic acid; In acetic acid;
DOI:10.1007/BF01175058

Reference yield:

: 17790-92-0
2,3,3-trimethyl-3H-indole hydrochloride

: 60878-55-9
10,10-dimethyl-10a-(4-diethylaminostyryl)-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-ones

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetic acid / 1 h / 100 °C

2: 93 percent / CH₃COOH,(CH₃CO)2O / 3 h / 100 °C

With acetic anhydride; acetic acid; In acetic acid;
DOI:10.1007/BF01175058