N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Base Information

Chemical Name:N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide
CAS No.:698973-53-4
Molecular Formula:C₂₂H₂₉NO₂Si
Molecular Weight:367.563
Hs Code.:

Synonyms:N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Suppliers and Price of N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

There total 4 articles about N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 696-62-8
para-iodoanisole

: 698973-51-2
N-cyclohexyl-N-(2-propynyl)-3-trimethylsilyl-2-propynamide

: 698973-53-4
N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 3173-53-3
Cyclohexyl isocyanate

: 698973-53-4
N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / -78 °C

1.2: tetrahydrofuran; hexane / 0.33 h / -78 °C

2.1: 2.48 g / tetrahydrofuran; hexane / 60 h / 20 °C

3.1: 81 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / tetrahydrofuran / 1 h / 20 °C

With copper(l) iodide; n-butyllithium; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane;

Reference yield:

: 910807-83-9
3-Trimethylsilanyl-propynoic acid cyclohexylamide

: 698973-53-4
N-cyclohexyl-N-[3-(4-methoxyphenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.48 g / tetrahydrofuran; hexane / 60 h / 20 °C

2: 81 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / tetrahydrofuran / 1 h / 20 °C

With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane;