[4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester

Base Information

• Chemical Name: [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester
• CAS No.: 158474-90-9
• Molecular Formula: C₁₉H₂₂F₆N₆O₄
• Molecular Weight: 512.412

Synonyms:[4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester

Chemical Property of [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester

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Technology Process of [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester

There total 3 articles about [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(4-azidophenyl)methyl 4-nitrophenoxyformate (161536-59-0) + N1,N8-bis(trifluoroacetyl)spermidinetriamine trifluoacetate → [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester (158474-90-9)

Guidance literature:

With iPrEtN; In tetrahydrofuran; at 25 ℃; for 24h;

DOI:10.1039/a806355i

Reference yield: 92.0%

N-[4-(trifluoroacetamido)butyl]-N-[3-(trifluoroacetamido)propyl]amine (158474-89-6) + (4-azidophenyl)methyl 4-nitrophenoxyformate (161536-59-0) → [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester (158474-90-9)

Guidance literature:

In tetrahydrofuran; for 24h; Ambient temperature;

DOI:10.1039/c39940002613

Reference yield:

N-(3-aminopropyl)-1,4-diaminobutane (124-20-9) → [4-(2,2,2-Trifluoro-acetylamino)-butyl]-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid 4-azido-benzyl ester (158474-90-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / H₂O / acetonitrile / 7 h

2: 92 percent / iPrEtN / tetrahydrofuran / 24 h / 25 °C

With water; In tetrahydrofuran; acetonitrile;

DOI:10.1039/a806355i

upstream raw materials:

N-[4-(trifluoroacetamido)butyl]-N-[3-(trifluoroacetamido)propyl]amine

(4-azidophenyl)methyl 4-nitrophenoxyformate

N-(3-aminopropyl)-1,4-diaminobutane

Downstream raw materials:

N⁴-(4-Azidobenzyloxycarbonyl)-N¹,N⁸-bis(nitroguanidino)spermidine

N-(4-guanidinylbutyl)-N-(3-guanidinylpropyl)amine

(4-Amino-butyl)-(3-amino-propyl)-carbamic acid 4-azido-benzyl ester

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