C₃₂H₃₅NO₃S

Base Information

Chemical Name:C₃₂H₃₅NO₃S
CAS No.:1374410-02-2
Molecular Formula:C₃₂H₃₅NO₃S
Molecular Weight:513.701
Hs Code.:

C<sub>32</sub>H<sub>35</sub>NO<sub>3</sub>S

Synonyms:C₃₂H₃₅NO₃S

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Chemical Property of C₃₂H₃₅NO₃S

Chemical Property:

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Technology Process of C₃₂H₃₅NO₃S

There total 5 articles about C₃₂H₃₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1374409-95-6
C₃₄H₃₇NO₄S

: 1374410-02-2
C₃₂H₃₅NO₃S

Guidance literature:: With diisobutylaluminium hydride; In hexanes; dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja302765m

Reference yield:

: 1374410-01-1
C₃₂H₃₅NO₄S

: 1374410-02-2
C₃₂H₃₅NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1: perchloric acid / tetrahydrofuran; water / 4 h / 22 °C / Inert atmosphere

2: tetrahydrofuran; toluene / 0 - 60 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 0 - 40 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate / toluene / 0.67 h / 80 °C / Inert atmosphere

5: diisobutylaluminium hydride / hexanes; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; perchloric acid; ammonium formate; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexanes; dichloromethane; water; toluene; 4: Tsuji reduction;
DOI:10.1021/ja302765m

Reference yield:

: 1374409-94-5
C₃₀H₃₁NO₄S

: 1374410-02-2
C₃₂H₃₅NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; toluene / 0 - 60 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0 - 40 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate / toluene / 0.67 h / 80 °C / Inert atmosphere

4: diisobutylaluminium hydride / hexanes; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexanes; dichloromethane; toluene; 3: Tsuji reduction;
DOI:10.1021/ja302765m