C₁₈H₂₃NO₅

Base Information

Chemical Name:C₁₈H₂₃NO₅
CAS No.:1265173-10-1
Molecular Formula:C₁₈H₂₃NO₅
Molecular Weight:333.384
Hs Code.:

C<sub>18</sub>H<sub>23</sub>NO<sub>5</sub>

Synonyms:C₁₈H₂₃NO₅

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Chemical Property of C₁₈H₂₃NO₅

Chemical Property:

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Technology Process of C₁₈H₂₃NO₅

There total 17 articles about C₁₈H₂₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1265173-09-8
C₂₉H₄₁NO₆Si

: 1265173-10-1
C₁₈H₂₃NO₅

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In water; acetonitrile; at 40 ℃; for 72h;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-20-3
C₂₂H₂₈O₇S

: 1265173-10-1
C₁₈H₂₃NO₅

Guidance literature:: Multi-step reaction with 12 steps

1.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C

2.1: toluene / 4 h / -40 °C

3.1: magnesium / methanol / 2 h / 20 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

5.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

5.2: 0 - 20 °C

6.1: pyridine / dichloromethane / 2 h / 0 °C

7.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

8.1: dichloromethane / 1 h / 0 °C

9.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

10.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

11.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

12.1: scandium tris(trifluoromethanesulfonate) / water; acetonitrile / 72 h / 40 °C

With pyridine; sulfur trioxide pyridine complex; acetic anhydride; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; toluene; acetonitrile; mineral oil; 4.1: Swern oxidation / 5.2: Horner-Wadsworth-Emmons olefination / 9.1: Overman rearrangement;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-04-3
C₂₃H₃₀O₇S

: 1265173-10-1
C₁₈H₂₃NO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: magnesium / methanol / 2 h / 20 °C

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

3.2: 0 - 20 °C

4.1: pyridine / dichloromethane / 2 h / 0 °C

5.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

6.1: dichloromethane / 1 h / 0 °C

7.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

8.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

9.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

10.1: scandium tris(trifluoromethanesulfonate) / water; acetonitrile / 72 h / 40 °C

With pyridine; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; toluene; acetonitrile; mineral oil; 2.1: Swern oxidation / 3.2: Horner-Wadsworth-Emmons olefination / 7.1: Overman rearrangement;
DOI:10.1002/asia.201000602