(5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

Base Information

• Chemical Name: (5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone
• CAS No.: 1597413-14-3
• Molecular Formula: C₂₅H₂₁N₃O₆
• Molecular Weight: 459.458

Synonyms:(5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

Chemical Property of (5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

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Technology Process of (5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone

There total 1 articles about (5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-2,7,8,13-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2,6-Pyridinedicarbonyl dichloride (3739-94-4) + N,N'-bis[(1S)-2-hydroxy-1-phenylethyl]ethanediamide → (5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-14-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; for 120h; Reflux;

DOI:10.1016/j.tetasy.2014.01.009

Reference yield:

(5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-14-3) + (S)-α-phenylethylamine hydrogen perchlorate (69128-54-7,73351-60-7,73395-23-0) → C25H21N3O6*C8H11N*ClHO4 (1597413-19-8)

Guidance literature:

In dimethylsulfoxide-d6; at 25 ℃;

DOI:10.1016/j.tetasy.2014.01.009

Reference yield:

(5S,10S)-5,10-diphenyl-3,12-dioxa-6,9,18-triazabicyclo[12.3.1]octadeca-1(18),14,16-triene-2,7,8,13-tetraone (1597413-14-3) + (R)-α-(1-naphthyl)ethylamine perchlorate salt (82456-17-5) → C25H21N3O6*C12H13N*ClHO4

Guidance literature:

In dimethylsulfoxide-d6; at 25 ℃;

DOI:10.1016/j.tetasy.2014.01.009

upstream raw materials:

2,6-Pyridinedicarbonyl dichloride

Downstream raw materials:

C₂₅H₂₁N₃O₆*C₈H₁₁N*ClHO₄

C₂₅H₂₁N₃O₆*C₈H₁₁N*ClHO₄

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