p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

Base Information

Chemical Name:p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate
CAS No.:156663-04-6
Molecular Formula:C₃₄H₂₉N₃O₅S
Molecular Weight:591.687
Hs Code.:

Synonyms:p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

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Chemical Property of p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

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Technology Process of p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

There total 11 articles about p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 156663-02-4
p-nitrobenzyl (2R)-3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-3-butenoate

: 156663-04-6
p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

Guidance literature:: With triethylamine; In dichloromethane; for 1.5h; Ambient temperature;

Reference yield: 11.0%

: 156663-08-0
2-[(2R,3R)-2-(2,5-Dioxo-pyrrolidin-1-ylsulfanyl)-4-oxo-3-(trityl-amino)-azetidin-1-yl]-3-methyl-but-2-enoic acid 4-nitro-benzyl ester

: 156663-04-6
p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

Guidance literature:: In toluene; for 5h; Heating;

Reference yield:

: 76-83-5
trityl chloride

: 156663-04-6
p-nitrobenzyl 3-methyl-2-(4-oxo-5-tritylimino-3-thiazolidynyl)-2-butenoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine / 1.) CH₂Cl₂, AcOH, RT, 2 h, 2.) CH₂Cl₂, AcOH, RT, 3 h

2: 2-Mercaptobenzothiazole / toluene / 5 h

3: triethylamine / dichloromethane / 1.5 h / Ambient temperature

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-Mercaptobenzothiazole; triethylamine; triphenylphosphine; In dichloromethane; toluene;