Technology Process of C59H89Cl2N3O15S
There total 6 articles about C59H89Cl2N3O15S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C60H91Cl2N3O15S;
With
sodium acetate;
In
methanol; water;
for 0.166667h;
With
iodine;
In
methanol; water;
at 60 ℃;
for 9h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tributylphosphine; water / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
1.2: 20 h / 20 °C / Inert atmosphere
2.1: methanol / 96 h / 20 °C
3.1: sodium acetate / methanol; water / 0.17 h
3.2: 9 h / 60 °C
With
methanol; tributylphosphine; water; sodium acetate;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium cyanoborohydride; acetic acid / methanol; water / 5 h / 28 °C
2.1: tributylphosphine; water / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
2.2: 20 h / 20 °C / Inert atmosphere
3.1: methanol / 96 h / 20 °C
4.1: sodium acetate / methanol; water / 0.17 h
4.2: 9 h / 60 °C
With
methanol; tributylphosphine; water; sodium acetate; sodium cyanoborohydride; acetic acid;
In
methanol; water; N,N-dimethyl-formamide;