pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃

Base Information

• Chemical Name: pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃
• CAS No.: 121566-69-6
• Molecular Formula: CHCl₃*C₄₅H₄₅CoN₅*ClO₄
• Molecular Weight: 933.708
• Mol file: 121566-69-6.mol

Synonyms:pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃

Chemical Property of pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃

There total 1 articles about pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

pentakis-(2,6-dimethylphenylisocyanide)cobalt(II) perchlorate hemihydrate → pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl3 (121566-69-6)

Guidance literature:

With CHCl₃; In pyridine; water; Co-complex dissolved in pyridine, allowed to stand (several min, room temp.), yellow-white residue removed by filtration, dropwise addn. of water, pptn., chilled thoroughly (ca 1 h), filtered, dried under suction (air), dissolved in CH3Cl; filtered through cotton, dropwise addn. of ether, pptn.;

DOI:10.1016/S0020-1693(00)80827-0

Reference yield:

pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * CHCl3 (121566-69-6) → pentakis-(2,6-dimethylphenylisocyanide)cobalt(I) perchlorate * 0.65CH2Cl2

Guidance literature:

With CH₂Cl₂; In diethyl ether; dichloromethane; Co-complex dissolved in CH2Cl2/ether; crystn., elem. anal.;

DOI:10.1016/S0020-1693(00)80827-0