C₅₅H₄₄FN₅O₉

Base Information

Chemical Name:C₅₅H₄₄FN₅O₉
CAS No.:1613589-46-0
Molecular Formula:C₅₅H₄₄FN₅O₉
Molecular Weight:937.981
Hs Code.:

C<sub>55</sub>H<sub>44</sub>FN<sub>5</sub>O<sub>9</sub>

Synonyms:C₅₅H₄₄FN₅O₉

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Chemical Property of C₅₅H₄₄FN₅O₉

Chemical Property:

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Technology Process of C₅₅H₄₄FN₅O₉

There total 17 articles about C₅₅H₄₄FN₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613589-43-7
C₃₄H₃₁N₅O₅

: 1613589-46-0
C₅₅H₄₄FN₅O₉

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 20 °C / Cooling with ice

2: dmap / dichloromethane / 0 - 20 °C

3: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C

With dmap; N-iodo-succinimide; 15-crown-5; triethylamine tris(hydrogen fluoride); In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1613589-44-8
C₃₄H₃₁FIN₅O₅

: 1613589-46-0
C₅₅H₄₄FN₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 0 - 20 °C

2: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C

With dmap; 15-crown-5; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1443997-54-3
(2R,3R,4R,5R)-5-((benzoyloxy)methyl)-3-ethynyltetrahydrofuran-2,3,4-triyl tribenzoate

: 1613589-46-0
C₅₅H₄₄FN₅O₉

Guidance literature:: Multi-step reaction with 9 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylsilyl trifluoromethanesulfonate / acetonitrile; toluene / 0 - 70 °C

2: silver nitrate / dichloromethane / 20 °C / Inert atmosphere

3: sodium ethanolate / 20 °C

4: pyridine / 16 h / 0 °C

5: sodium iodide / acetone / Reflux

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 60 °C

7: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 20 °C / Cooling with ice

8: dmap / dichloromethane / 0 - 20 °C

9: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C

With pyridine; dmap; N-iodo-succinimide; 15-crown-5; trimethylsilyl trifluoromethanesulfonate; sodium ethanolate; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;