Technology Process of C32H44N2O5Si
There total 2 articles about C32H44N2O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonamide; hydroquinidein 1,4-phthalazinediyl diether;
In
water; tert-butyl alcohol;
at 4 ℃;
for 72h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.066
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine; dmap / 0.75 h / 0 - 20 °C / Inert atmosphere
2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
2.2: 12 h / -65 °C / Inert atmosphere
3.1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice; Inert atmosphere
4.1: pyridine / 1.5 h / 0 - 20 °C / Inert atmosphere
5.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
6.1: methanesulfonamide; hydroquinidein 1,4-phthalazinediyl diether / water; tert-butyl alcohol / 72 h / 4 °C / Inert atmosphere
With
pyridine; dmap; sodium tetrahydroborate; n-butyllithium; methanesulfonamide; potassium tert-butylate; hydroquinidein 1,4-phthalazinediyl diether; diisopropylamine;
In
tetrahydrofuran; methanol; hexane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2010.12.066
- Guidance literature:
-
C32H44N2O5Si;
With
Trimethyl orthoacetate; pyridinium p-toluenesulfonate;
In
dichloromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
With
chloro-trimethyl-silane;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.066
