5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

Base Information

Chemical Name:5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene
CAS No.:1422960-21-1
Molecular Formula:C₄₀H₂₀Cl₄
Molecular Weight:642.411
Hs Code.:

Synonyms:5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

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Chemical Property of 5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

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Technology Process of 5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

There total 2 articles about 5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1422960-18-6
5,6-bis[(2,6-dichlorophenyl)ethynyl]-1,2-dihydroacenaphthylene

: 83-32-9
acenaphthene

: 1422960-21-1
5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

Guidance literature:: 5,6-bis[(2,6-dichlorophenyl)ethynyl]-1,2-dihydroacenaphthylene; acenaphthene; With tris(triphenylphosphine)rhodium(l) chloride; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 60h; Inert atmosphere; Sealed tube;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 5h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201208200

Reference yield: 70.0%

: 1422960-18-6
5,6-bis[(2,6-dichlorophenyl)ethynyl]-1,2-dihydroacenaphthylene

: 208-96-8,25036-01-5
acenaphthylene

: 1422960-21-1
5,12-bis(2,6-dichlorophenyl)-1,2-dihydroacenaphtho[1,2-k]cyclopenta[cd]fluoranthene

Guidance literature:: 5,6-bis[(2,6-dichlorophenyl)ethynyl]-1,2-dihydroacenaphthylene; acenaphthylene; With Wilkinson's catalyst; In para-xylene; at 130 ℃; for 60h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone;
DOI:10.1002/chem.201303357