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3-butenal dibenzylacetal

Base Information
  • Chemical Name:3-butenal dibenzylacetal
  • CAS No.:223906-12-5
  • Molecular Formula:C18H20O2
  • Molecular Weight:268.356
  • Hs Code.:
3-butenal dibenzylacetal

Synonyms:3-butenal dibenzylacetal

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Chemical Property of 3-butenal dibenzylacetal
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Technology Process of 3-butenal dibenzylacetal

There total 1 articles about 3-butenal dibenzylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With pyridinium p-toluenesulfonate; In benzene; for 4.5h; Heating;
DOI:10.1021/ja9842464
Guidance literature:
With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja9842464
Guidance literature:
Multi-step reaction with 2 steps
1: 55 percent / MCPBA / CH2Cl2
2: 1.) BuLi, 2.) Me3Al / 1.) toluene, hexane, 0 deg C, 3 h, 2.) toluene, hexane, 25 deg C, 12 h
With n-butyllithium; trimethylaluminum; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja9842464
upstream raw materials:

3-butenal 1,1-diethylacetal

benzyl alcohol

Downstream raw materials:

2-(2,2-bis-benzyloxy-ethyl)-oxirane

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